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2.5F: Sample Preparation for Gas Chromatography Apr 7, 2022 · Add one or two “specks” of solid 16 (a pile approximately 2 mm in diameter), or a very small spatula-tip of solid to a GC vial (Figure 2.93c). Then add a low boiling solid (e.g. methanol, clean acetone, diethyl ether, or dichloromethane) to the 1.5 mL mark. Cap the vial and invert several times to fully dissolve the solid. Autosampler Vials, Inserts, and Closures | Fisher Scientific Gas Chromatograph-Mass Spectrometr...

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